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A New and Convenient Method of Generating Alkyl Isocyanates from Alcohols, Thiols, and Trimethylsilyl Ethers Using a 2,4,6-Trichloro[1,3,5] Triazine/n-Bu4NOCN
2,4,6-Trichloro[1,3,5] triazine (TT) alcohol thiol trimethylsilyl ether alkyl isocyanate
2010/4/19
Alkyl isocyanates are prepared in good to excellent yields by treatment of alcohols, thiols, and trimethylsilyl ethers with 2,4,6-trichloro[1,3,5] triazine/n-Bu4NOCN in acetonitrile. This method is hi...